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When montmorillonite is treated with a metal salt in organic solvents, impregnation occurs instead of ion exchange The first highly successful catalytic material prepared by supporting ZnCl 2 from methanol solution to KlO montmorillonite was called "clayzic" 140 Clayzic exhibits activities which are several orders of magnitude higher than those of the ion-exchanged materials and can induce FriedelCrafts alkylations with alcohols, alkyl halides and aldehydes 85 Since the development of clayzic, other montmorillonite-supported catalysts were also prepared and studied New examples are montmorillonites modified with FeCl 3 or SbCl3 from acetonitrile solution that show good characteristics in the alkylation of arenes with benzyl chloride 86,387 The performance of the catalyst modified with SbCl 3 is especially surprising considering the low activity of this weak Lewis acid under homogeneous conditions.

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ZnCl 2 supported on hydroxyapatite promotes selective monoalkylation of benzene, toluene, and p-xylene by benzyl chloride,388 whereas AICl 3 and ZnCl 2 supported on MCM-41 are promising catalysts in the formation of diphenylmethane 89 An immobilized form of AICl 3 using porous materials, including Si02, A1 20 3, and KlO, which displays high activity in the liquid phase, was reported 90 AIkenes and chloroalkanes react smoothly under mild conditions Activities are comparable to that of AICI 3, and selectivities are often better The catalysts can be recycled without loss of activity and selectivity AICl 3 could also be immobilized on MCM_41 391 When used in the alkylation of benzene with C6-C 16 linear l-alkenes, this novel shape-selective material with optimal pore size always exhibited better selectivities toward monosubstituted linear alkylbenzenes than AICl 3 in the homogeneous phase.

A significant increase in the selectivity toward 2,6-diisopropylnaphthalene could be achieved with a similar catalyst prepared with external surface-silylated MCM-41 392 MCM-41 was found to be an ideal support to prepare highly active and reusable supported Ga203, In203, GaCl 3, and InCl 3 catalysts for the benzylation of methylbenzenes 93 ZnCl 2 supported in sol-gel-derived silica394 or aluminosilicates395 is effective in Friedel-Crafts alkylations Significantly higher activities than over commercially available clayzic were observed, which were correlated with high total pore volume Sulfated zirconia catalysts showed selectivities comparable to those of AICl 3 in the alkylation of benzene with l-alkenes to linear alkylbenzenes 96 The mesoporous sulfated zirconia sample could be regenerated by solvent extraction or thermal treatment.

To delete a series name, use the Source Data dialog box as described previously. Select the series name to delete; then, highlight the range reference (or text) in the Name box and press Del. Alternatively, you can edit the SERIES formula and remove the first argument. Here s an example of a SERIES formula for a series with no specified name (it will use the default name):

Phosphotungstic acid supported on sulfated zirconia doped with Fe proved to be very active and highly selective in the alkylation of benzene with propylene at 100-150 C to produce cumene; both monoalkylation and cumene formation have better than 90% selectivity 97 It can be regenerated at moderate temperature (350 C) The solid acid catalyzed adamantylation of substituted benzene derivatives was studied with the aim to achieve high para regioselectivities Of various acidic resins, zeolite HY, sulfated zirconia, perfluorolkanesulfonic acids, and phosphotungstic acid, Ambedyst XN-lOlO was found to be the catalyst of choice to afford para-substituted alkylbenzenes with selectivities exceeding 70% 98 In further systematic studies with a Nafion-H-silica nanocomposite catalyst,399 and various.

the entire vessel. The time constants, , for low and high Sc are taken from Table 2-4. The macroscale of mixing, Ls , is not well established, so estimates for this, and for , are needed. Brodkey (1967, p. 351) suggests 5

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